Unique Pesticide Analysis Method

contributed by SCIEX | 03/24/2016

Comprehensive Quantitation and Identification of Pesticides in Food Samples using LC-MS/MS with Scheduled MRM™, Fast Polarity Switching, and MS/MS Library Searching

Liquid Chromatography coupled to Tandem Mass Spectrometry (LC-MS/MS) is a widely used analytical tool for the screening of food residues and contaminants. Here, we present a new and unique method using QuEChERS extraction, separation using a polar embedded C18 phase, and MS/MS detection with highly selective and sensitive Multiple Reaction Monitoring (MRM) on an SCIEX QTRAP® 5500 system. The Scheduled MRM algorithm was used to obtain the best data quality and combined with fast polarity switching to cover the broadest range of pesticides possible. In addition MS/MS spectra were acquired to enable compound identification with highest confidence based on mass spectral library matching.

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M. Anastassiades, et al.: J. AOAC Int. 86 (2003) 412-431
A. Schreiber and RebeccaWittrig.: AgroFOOD 21 (2010) 16- 19
J. Wong et al.: J. Agric. Food Chem. 58 (2010) 5897-5903
A. Schreiber and Nadia Pace.: Application Note SCIEX (2010) 1282310-01
K. von Czapiewski et al.: Application Note SCIEX (2011) 2110211-01
A. Schreiber et al.: Application Note SCIEX (2010) 1121010-01